Αποτελέσματα Αναζήτησης
4 Φεβ 2020 · This can increase yield and average product size by for instance decreasing temperature or increasing antisolvent fraction (Figure. 1.11) in each cascade crystallizer while keeping relatively mild supersaturation conditions to avoid crystal nucleation and promote crystal growth in the subsequent crystallizers. Note that for a cascade of (well ...
In making the material balances, the calculations are straightforward when the solute crystals are anhydrous. Simple water and solute material balances are made. When the crystallizations are hydrated, some of the water in solution is removed with the crystals as a hydrate. Yield of a Crystallization Process.
Crystallization is the process of forming a crystalline material from a liquid, gas or amorphous solid. The crystals thus formed have highly regular internal structure, the basis of which is called the crystal lattice. Since the formation of such a highly ordered structure prohibits
A loss of recovery should be expected when performing a crystallization. Although there are ways to maximize the return of crystals, a portion of the desired compound will always be lost. The reasons for this are both inherent to the design of the process and mechanical.
Reading through an analytical textbook, it states a few ways to improve yield and purity but it doesn't actually state how you would do it practically: allow the solution cool down as slowly as possible. This will maximize crystal size. maintain a low relative supersaturation of the solution, this will increase crystal size and improve purity
4 Ιαν 2014 · If the yield from either of the processes is low, then a second solvent can be added to reduce the effectiveness of the first and thus decrease the residual solution concentration (sometimes called ‘drowning-out’ or ‘watering-out’).
2 Φεβ 2011 · Crystallization is used industrially in a wide variety of processes. Typical applications include bulk chemicals, such as salt, sugar and fertilizers; high value-added products such as specialty chemicals and pharmaceuticals; and difficult separations such as ortho- and para-xylene.
