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The XRD analysis of the prepared sample of TiO 2 nanoparticles was done using a Bruker make diffractometer, Cu-Kα X-rays of wavelength (λ)=1.5406 Å and data was taken for the 2 θ range of 10° to 70° with a step of 0.1972°.
Download scientific diagram | XRD patterns for rutile, anatase, and mixed TiO2 phases. The JCPDS #75-1537 for TiO2 is shown as a reference.
The XRD patterns of the three main crystalline phases of TiO 2 are reported in Figure ... View in full-text. Context 2. ... microscopies SEM and TEM are local techniques and should be used...
1 Ιουλ 2013 · Morphology index (MI) derived from FWHM of XRD data explains the interrelationship of particle size and specific surface area. It is observed that MI has direct relationship with particle size...
23 Ιουλ 2019 · X-ray diffraction (XRD) patterns for samples of nanoparticles having different sizes and shapes can look different, and careful analysis of the XRD data can provide useful information and also help correlate microscopic observations with the bulk sample.
23 Ιουλ 2019 · Analysis of a sample by powder XRD provides important information that is complementary to various microscopic and spectro-scopic methods, such as phase identi cation, sample purity, fi crystallite size, and, in some cases, morphology.
1 Ιουλ 2022 · Abstract. For more than 20 years, Pt/TiO 2 represents the benchmark photocatalyst/co-catalyst platform for photocatalytic hydrogen (H 2) generation. Here, single atom (SA) Pt is decorated on different polymorphs of TiO 2 (anatase, rutile, and the mixed phase of P25) using a simple immersion anchoring approach.